US2440555A - Abietate ester hair dressing - Google Patents
Abietate ester hair dressing Download PDFInfo
- Publication number
- US2440555A US2440555A US472160A US47216043A US2440555A US 2440555 A US2440555 A US 2440555A US 472160 A US472160 A US 472160A US 47216043 A US47216043 A US 47216043A US 2440555 A US2440555 A US 2440555A
- Authority
- US
- United States
- Prior art keywords
- abietate
- hair
- ester
- hair dressing
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- -1 Abietate ester Chemical class 0.000 title description 6
- BTXXTMOWISPQSJ-UHFFFAOYSA-N 4,4,4-trifluorobutan-2-one Chemical compound CC(=O)CC(F)(F)F BTXXTMOWISPQSJ-UHFFFAOYSA-N 0.000 description 8
- 239000003676 hair preparation Substances 0.000 description 8
- BQACOLQNOUYJCE-FYZZASKESA-N Abietic acid Natural products CC(C)C1=CC2=CC[C@]3(C)[C@](C)(CCC[C@@]3(C)C(=O)O)[C@H]2CC1 BQACOLQNOUYJCE-FYZZASKESA-N 0.000 description 7
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 7
- OVXRPXGVKBHGQO-UYWIDEMCSA-N methyl (1r,4ar,4br,10ar)-1,4a-dimethyl-7-propan-2-yl-2,3,4,4b,5,6,10,10a-octahydrophenanthrene-1-carboxylate Chemical compound C1CC(C(C)C)=CC2=CC[C@H]3[C@@](C(=O)OC)(C)CCC[C@]3(C)[C@H]21 OVXRPXGVKBHGQO-UYWIDEMCSA-N 0.000 description 7
- 238000001035 drying Methods 0.000 description 6
- 150000002148 esters Chemical class 0.000 description 6
- 235000019441 ethanol Nutrition 0.000 description 6
- 229940023878 hydrogenated methyl abietate Drugs 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- RSWGJHLUYNHPMX-ONCXSQPRSA-N abietic acid Chemical class C([C@@H]12)CC(C(C)C)=CC1=CC[C@@H]1[C@]2(C)CCC[C@@]1(C)C(O)=O RSWGJHLUYNHPMX-ONCXSQPRSA-N 0.000 description 4
- 230000001476 alcoholic effect Effects 0.000 description 4
- 239000000975 dye Substances 0.000 description 4
- 210000004761 scalp Anatomy 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
- OVXRPXGVKBHGQO-UHFFFAOYSA-N abietic acid methyl ester Natural products C1CC(C(C)C)=CC2=CCC3C(C(=O)OC)(C)CCCC3(C)C21 OVXRPXGVKBHGQO-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- MTHSVFCYNBDYFN-UHFFFAOYSA-N anhydrous diethylene glycol Natural products OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 230000001681 protective effect Effects 0.000 description 2
- 239000000344 soap Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- AGUBCDYYAKENKG-UHFFFAOYSA-N Abietinsaeure-aethylester Natural products C1CC(C(C)C)=CC2=CCC3C(C(=O)OCC)(C)CCCC3(C)C21 AGUBCDYYAKENKG-UHFFFAOYSA-N 0.000 description 1
- AGUBCDYYAKENKG-YVNJGZBMSA-N Ethyl abietate Chemical compound C1CC(C(C)C)=CC2=CC[C@H]3[C@@](C(=O)OCC)(C)CCC[C@]3(C)[C@H]21 AGUBCDYYAKENKG-YVNJGZBMSA-N 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 239000002313 adhesive film Substances 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 239000000834 fixative Substances 0.000 description 1
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
Definitions
- the present invention relates to hair preparations, and more particularly to a preparation having utility as a hair dressing.
- the object of the present invention is to provide a new and improved hair preparation which is made from comparatively inexpensive and easily available materials; which has a viscosity high enough to maintain the hair straight, dressed and well-groomed; which imparts an attractive gloss to the hair; which has a color well suited for hair dressing; which has a nonobjectionable odor; which does not develop rancidity; which is non-drying and therefore maintains the hair soft; which forms a thin protective non-tacky adhesive film of non-greasy characteristics on the hair; and which can be readily washed off with soap and water.
- an aliphatic alcoholic ester of abietic acid such as methyl abietate or a hydrogenated alcoholic ester of abietic acid such as methyl abietate hydrogenated is employed as an ingredient of the hair preparation.
- a 30% hydrogenated methyl abietate has been found particularly suited for this purpose.
- This abietate which is comparatively inexpensive and easily available, is soluble in alcohol, and forms there- With a clear solution which does not turn cloudy when cooled to C.
- this abietate has a very high viscosity which enables it to keep the hair in place, straight and well-groomed; it has a very pale yellow color which is suitable for commercial hair preparations; it has a slight non-objectionable odor and unlike vegetable oils does not develop rancidity on standing; it im-- parts an attractive luster to the hair; it is substantially non-drying so that the hair does not become stiff, but appears soft; it forms a thin protective adhesive non-tacky, non-greasy film which covers the hair and scalp and prevents loss of scalp oils and consequent dryness of the scalp; and it can be readily washed off the scalp with soap and Water.
- a 30% hydrogenated methyl abietate is dissolved in isopropyl, ethyl, butyl alcohol or other harmless, volatile solvents.
- This abietate may constitute 3 to 50% of the preparation.
- composition may, for example, comprise about 10% of 30% hydrogenated methyl abietate and about 90% ethyl alcohol. This preparation may have perfume added to it.
- esters of abietic acid which may be used in accordance with the present invention are ethyl abietate, ethylene glycol ester of abietic acid. diethylene glycol ester of abietic 5 acid, triethylene glycol ester of abietlc acid and glycerol ester of abietic acid. These esters may be of hydrogenated or non-hydrogenated abietic acid, and when adjusted in solution with alcohol or other volatile solvents, produce an eifective hair dressing preparation.
- a non-drying hair preparation free from dyes comprising essentially an alcohol solution of 3 to 50% of about 30% hydrogenated methyl 30 abietate.
- a non-drying hair preparation free from dyes comprising essentially about of about hydrogenated methyl abietate in alcohol solution. ALLEN L. OMOHUNDRO.
Description
Patented Apr. 27, 1948 UNITED STATES ABIETATE ESTER HAIR DRESSING Allen L. Omohundro, Wilton,
Fairfield, Conn,
and Emil C. Fanto,
assignors to McKesson & Robbins, Incorporated, Bridgeport, Conn., a corporation of Maryland No Drawing. Application January 12, 1943, Serial No. 472,160
4 Claims. 1
The present invention relates to hair preparations, and more particularly to a preparation having utility as a hair dressing.
The object of the present invention is to provide a new and improved hair preparation which is made from comparatively inexpensive and easily available materials; which has a viscosity high enough to maintain the hair straight, dressed and well-groomed; which imparts an attractive gloss to the hair; which has a color well suited for hair dressing; which has a nonobjectionable odor; which does not develop rancidity; which is non-drying and therefore maintains the hair soft; which forms a thin protective non-tacky adhesive film of non-greasy characteristics on the hair; and which can be readily washed off with soap and water.
In carrying out the features of the present invention, an aliphatic alcoholic ester of abietic acid such as methyl abietate or a hydrogenated alcoholic ester of abietic acid such as methyl abietate hydrogenated is employed as an ingredient of the hair preparation. A 30% hydrogenated methyl abietate has been found particularly suited for this purpose. This abietate, which is comparatively inexpensive and easily available, is soluble in alcohol, and forms there- With a clear solution which does not turn cloudy when cooled to C. Furthermore, this abietate has a very high viscosity which enables it to keep the hair in place, straight and well-groomed; it has a very pale yellow color which is suitable for commercial hair preparations; it has a slight non-objectionable odor and unlike vegetable oils does not develop rancidity on standing; it im-- parts an attractive luster to the hair; it is substantially non-drying so that the hair does not become stiff, but appears soft; it forms a thin protective adhesive non-tacky, non-greasy film which covers the hair and scalp and prevents loss of scalp oils and consequent dryness of the scalp; and it can be readily washed off the scalp with soap and Water.
As a specific example of a preparation which is found suitable in accordance with the present invention a 30% hydrogenated methyl abietate is dissolved in isopropyl, ethyl, butyl alcohol or other harmless, volatile solvents. This abietate may constitute 3 to 50% of the preparation. A
' specific composition may, for example, comprise about 10% of 30% hydrogenated methyl abietate and about 90% ethyl alcohol. This preparation may have perfume added to it.
2 Other alcoholic esters of abietic acid which may be used in accordance with the present invention are ethyl abietate, ethylene glycol ester of abietic acid. diethylene glycol ester of abietic 5 acid, triethylene glycol ester of abietlc acid and glycerol ester of abietic acid. These esters may be of hydrogenated or non-hydrogenated abietic acid, and when adjusted in solution with alcohol or other volatile solvents, produce an eifective hair dressing preparation.
We have described what We believe to :be the best embodiments of our lnventiom We do not wish, however, to be confined to the embodiments shown, but what we desire to cover by Letters Patent is set forth in the appended claims.
We claim:
1. A non-drying hair preparation free from dyes, and containing essentially an alcoholic solution of a hair fixative ingredient of the class consisting of the esters of abietic acid and the hydrogenated esters of abietic acid in proportions of 3 to 50% 2. A non-drying hair preparation free from dyes and comprising essentially an alcohol solution of hydrogenated methyl abietate in proportions of 3 to 50%.
3. A non-drying hair preparation free from dyes comprising essentially an alcohol solution of 3 to 50% of about 30% hydrogenated methyl 30 abietate.
4. A non-drying hair preparation free from dyes comprising essentially about of about hydrogenated methyl abietate in alcohol solution. ALLEN L. OMOHUNDRO.
EMIL C. FANTO.
REFERENCES CITED The following references are of record in the file of this patent:
UNITED STATES PATENTS Number Name Date 1,167,264 Brooks Jan. 4, 1916 1,682,280 Johnston Aug. 28,, 1928 2,230,063 Klimlst Jan. 28,, 1941 OTHER REFERENCES Hercolyn, published by Hercules Powder Co.,
July 1938, Pa e 3.
Manufacturing Chemist, Oct. 1940, page 266. Am. J. Pharm, Oct. 1936, page 434.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US472160A US2440555A (en) | 1943-01-12 | 1943-01-12 | Abietate ester hair dressing |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US472160A US2440555A (en) | 1943-01-12 | 1943-01-12 | Abietate ester hair dressing |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US2440555A true US2440555A (en) | 1948-04-27 |
Family
ID=23874423
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US472160A Expired - Lifetime US2440555A (en) | 1943-01-12 | 1943-01-12 | Abietate ester hair dressing |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US2440555A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4128543A (en) * | 1977-01-24 | 1978-12-05 | Inolex Corporation | Process for preparing alcohol soluble condensates of abietic acid and a protein hydrolysate |
| US4229429A (en) * | 1978-09-20 | 1980-10-21 | Inolex Corporation | Process for preparing alcohol soluble condensates of abietic acid and a protein hydrolsate |
| US5935561A (en) * | 1996-03-27 | 1999-08-10 | Procter & Gamble Company | Conditioning shampoo compositions containing select hair conditioning agents |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1167264A (en) * | 1914-12-02 | 1916-01-04 | Gulf Refining Co | Stable rosin and process of making the same. |
| US1682280A (en) * | 1928-08-28 | Alan c | ||
| US2230063A (en) * | 1939-01-23 | 1941-01-28 | Martin Gordon M | Liquid lip rouge preparation |
-
1943
- 1943-01-12 US US472160A patent/US2440555A/en not_active Expired - Lifetime
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1682280A (en) * | 1928-08-28 | Alan c | ||
| US1167264A (en) * | 1914-12-02 | 1916-01-04 | Gulf Refining Co | Stable rosin and process of making the same. |
| US2230063A (en) * | 1939-01-23 | 1941-01-28 | Martin Gordon M | Liquid lip rouge preparation |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4128543A (en) * | 1977-01-24 | 1978-12-05 | Inolex Corporation | Process for preparing alcohol soluble condensates of abietic acid and a protein hydrolysate |
| US4229429A (en) * | 1978-09-20 | 1980-10-21 | Inolex Corporation | Process for preparing alcohol soluble condensates of abietic acid and a protein hydrolsate |
| US5935561A (en) * | 1996-03-27 | 1999-08-10 | Procter & Gamble Company | Conditioning shampoo compositions containing select hair conditioning agents |
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