CN105250159A - Lasting lip gloss and preparation method thereof - Google Patents

Lasting lip gloss and preparation method thereof Download PDF

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Publication number
CN105250159A
CN105250159A CN201510642689.2A CN201510642689A CN105250159A CN 105250159 A CN105250159 A CN 105250159A CN 201510642689 A CN201510642689 A CN 201510642689A CN 105250159 A CN105250159 A CN 105250159A
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CN
China
Prior art keywords
lip gloss
weight portion
polymethylsilsesquioxane
skin conditioning
gloss according
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201510642689.2A
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Chinese (zh)
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CN105250159B (en
Inventor
何廷刚
何志泉
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hua An Tang biotech Group Co., Ltd.
Original Assignee
City Flower An Tang Bio Tech Ltd Guangzhou
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Priority to CN201510642689.2A priority Critical patent/CN105250159B/en
Publication of CN105250159A publication Critical patent/CN105250159A/en
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Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/342Alcohols having more than seven atoms in an unbroken chain
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02Preparations containing skin colorants, e.g. pigments
    • A61Q1/04Preparations containing skin colorants, e.g. pigments for lips
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/001Preparations for care of the lips

Abstract

The invention belongs to the technical field of cosmetics, and particularly relates to lasting lip gloss and a preparation method thereof. The lip gloss is prepared from emollient, skin conditioning agents, a thickener, an antioxidant and a colorant. The colorant is composed of polymethylsilsesquioxane and CII 2490. The skin conditioning agent comprises bisabolol and farnesol. The lip gloss can keep stable and does not fade after being irradiated by outdoor sunshine, indoor fluorescent lamps and other light sources. The lip gloss is long in shelf life, unchanged in appearance and more stable in quality. The lip gloss can be scattered in a formula by being added into the formula and stirred or subjected to low-speed homogenization, and has heat resistance. Production efficiency is greatly improved, and the problems of losses, color difference and the like are reduced.

Description

A kind of lasting color lip gloss and preparation method thereof
Technical field
The invention belongs to cosmetic technical field, be specifically related to a kind of lasting color lip gloss and preparation method thereof.
Background technology
All the time, color make-up product particularly ruddy product after outdoor solar light, indoor day light source irradiation such as illuminator, there will be COLOR FASTNESS PROBLEM in various degree.General solution adds the light stabilizers such as sunscreen in formula, but weak effect, formulation stability is also bad.Pigment dispersion is the important step of color make-up product in preparation and the problem of emphasis needs solution.The process for dispersing of tradition pigment has two kinds: (1) uses oils and fats and pigment premixing, scattered through the mixing apparatus such as three-roll grinder or ball grinding, then joins in formula.(2) use the powder class raw material used in formula and pigment premixing, be casually arranged with through miniature high-speed dispersion machine decile standby scattered, then join in formula.No matter be which kind of method above, all need first pre-dispersed pigments just can add in formula.Cause production efficiency low, loss is large, and aberration is large waits series of problems.
Color make-up comprises lip gloss, and lip gloss is thick liquid or thin body paste, be rich in all kinds of height moisten oils and fats and flash of light the factor, contained waxiness and color pigments few.Bright exquisitely carved, moisten frivolous; Make the moistening third dimension of lips strong after colouring; Especially pursue special dress up effect time have outstanding performance.Be the lip gloss that market is sold now, major part is all easily faded (de-adornment).
Therefore, the problem of fading of coloring agent in lip gloss is that cosmetics researcher needs one of difficult point urgently to be resolved hurrily always.
Summary of the invention
For these reasons, applicant is through years of researches, for solving the problem of lip products light fading, add trace organosilicon, bisabolol and farnesol in lip gloss, this lip gloss can also keep stablizing after outer sunlight, indoor day light source irradiation such as illuminator colour-fast.Make the shelf life of product longer, perception remains unchanged, and quality is more stable.This lip gloss only needs to stir or low speed homogenizing just dispersibles in formula adding in formula, and has heat resistance.Substantially increase production efficiency, the problem such as Loss reducing and aberration.
The present invention is achieved through the following technical solutions.
A kind of lip gloss, be prepared from by emollient, skin conditioning agent, thickening agent, antioxidant and coloring agent, coloring agent is made up of polymethylsilsesquioxane and CI12490, and skin conditioning agent comprises bisabolol and farnesol.
Described a kind of lip gloss, wherein emollient 100-110 weight portion, skin conditioning agent 9-13 weight portion, thickening agent 8-10 weight portion, antioxidant 1-1.5 weight portion, coloring agent 1.5-2.5 weight portion.
Described a kind of lip gloss, wherein emollient 105 weight portion, skin conditioning agent 11 weight portion, thickening agent 9 weight portion, antioxidant 1.2 weight portion, coloring agent 2 weight portion.
Described a kind of lip gloss, wherein the weight ratio of polymethylsilsesquioxane and CI12490 is 1.98:0.02.
Described a kind of lip gloss, wherein bisabolol and farnesol weight ratio are 1:1.
Described a kind of lip gloss, wherein emollient is hydrogenated polydecene, tridecyl alcohol trimellitate, two-two glycerol many acyl groups adipate esters-2, Fructus oleae europaeae fruit oil, behenyl alcohol.
Described a kind of lip gloss, wherein skin conditioning agent squalane, Jojoba seed oil.
Described a kind of lip gloss, wherein thickening agent dimetylsilyl SiClx stone, polyethylene.
Described a kind of lip gloss, wherein anti-oxidant tocopherol acetas, butylated hydroxytoluene.
Following is preferred lip gloss prescription
Described a kind of lip gloss, wherein the preparation method of lip gloss is:
Hydrogenated polydecene, tridecyl alcohol trimellitate, two-two glycerol many acyl groups adipate esters-2, Fructus oleae europaeae fruit oil, squalane, behenyl alcohol, Jojoba seed oil, polyethylene, tocopherol acetas, bisabolol, farnesol are mixed and heated to 90-95 DEG C and melt completely; Add dimetylsilyl SiClx stone, complete with homogenizer homogenizing; Add polymethylsilsesquioxane, CI12490, dispersed with stirring is complete; Be filled to when 90-95 DEG C in packaging material, obtain lip gloss.
The present invention has following useful technique effect:
1, by adding polymethylsilsesquioxane, CI12490, bisabolol, farnesol, thus ensure that lip gloss is stablized, colour-fast within a certain period of time.
2, the component content added is lower, but does not need special process, only needs to stir or low speed homogenizing, and has heat resistance.
3, whole technology preparation is simple, is applicable to suitability for industrialized production, enhances productivity.
Detailed description of the invention
Below in conjunction with example, the present invention is elaborated.Following examples do not limit protection scope of the present invention.
One, organosilicon addition test
Test according to following prescription:
Test 1 group: polymethylsilsesquioxane 1g, CI124901g;
Test 2 groups: polymethylsilsesquioxane 1.5g, CI124900.5g;
Test 3 groups: polymethylsilsesquioxane 1.8g, CI124900.2g;
Test 4 groups: polymethylsilsesquioxane 1.9g, CI124900.1g;
Test 5 groups: polymethylsilsesquioxane 1.98g, CI124900.02g;
The method that above-mentioned test group is prepared into lip gloss is: hydrogenated polydecene, tridecyl alcohol trimellitate, two-two glycerol many acyl groups adipate esters-2, Fructus oleae europaeae fruit oil, squalane, behenyl alcohol, Jojoba seed oil, polyethylene, tocopherol acetas, bisabolol, farnesol are mixed and heated to 90-95 DEG C and melt completely; Add dimetylsilyl SiClx stone, complete with homogenizer homogenizing; Add polymethylsilsesquioxane, CI12490, dispersed with stirring is complete; Be filled to when 90-95 DEG C in packaging material, obtain lip gloss.
Test method: get above-mentioned different lip gloss, irradiate under being placed on D65 illumination, observe artificial fading time.
Result of the test: in table 1.
The fading time of the different lip gloss of table 1
Note: enterprise marks: lip gloss faded defective lower than 5 days.
Conclusion (of pressure testing): above-mentioned test shows, the part by weight relation of polymethylsilsesquioxane and CI12490, for fading time important, and as polymethylsilsesquioxane and itself 1.9:0.1 or 1.98:0.02 of CI12490 weight ratio, lip gloss fading time conforms to quality requirements (being greater than 5 days).
Two, bisabolol and farnesol are on the impact of lip gloss
Test 1 group:
Preparation method: hydrogenated polydecene, tridecyl alcohol trimellitate, two-two glycerol many acyl groups adipate esters-2, Fructus oleae europaeae fruit oil, squalane, behenyl alcohol, Jojoba seed oil, polyethylene, tocopherol acetas, bisabolol are mixed and heated to 90-95 DEG C and melt completely; Add dimetylsilyl SiClx stone, complete with homogenizer homogenizing; Add polymethylsilsesquioxane, CI12490, dispersed with stirring is complete; Be filled to when 90-95 DEG C in packaging material, obtain lip gloss.
Test 2 groups:
Preparation method: hydrogenated polydecene, tridecyl alcohol trimellitate, two-two glycerol many acyl groups adipate esters-2, Fructus oleae europaeae fruit oil, squalane, behenyl alcohol, Jojoba seed oil, polyethylene, tocopherol acetas, farnesol are mixed and heated to 90-95 DEG C and melt completely; Add dimetylsilyl SiClx stone, complete with homogenizer homogenizing; Add polymethylsilsesquioxane, CI12490, dispersed with stirring is complete; Be filled to when 90-95 DEG C in packaging material, obtain lip gloss.
Test 3 groups:
Hydrogenated polydecene, tridecyl alcohol trimellitate, two-two glycerol many acyl groups adipate esters-2, Fructus oleae europaeae fruit oil, squalane, behenyl alcohol, Jojoba seed oil, polyethylene, tocopherol acetas, bisabolol, farnesol are mixed and heated to 90-95 DEG C and melt completely; Add dimetylsilyl SiClx stone, complete with homogenizer homogenizing; Add polymethylsilsesquioxane, CI12490, dispersed with stirring is complete; Be filled to when 90-95 DEG C in packaging material, obtain lip gloss.
Test 4 groups:
Hydrogenated polydecene, tridecyl alcohol trimellitate, two-two glycerol many acyl groups adipate esters-2, Fructus oleae europaeae fruit oil, squalane, behenyl alcohol, Jojoba seed oil, polyethylene, tocopherol acetas, bisabolol, farnesol are mixed and heated to 90-95 DEG C and melt completely; Add dimetylsilyl SiClx stone, complete with homogenizer homogenizing; Add polymethylsilsesquioxane, CI12490, dispersed with stirring is complete; Be filled to when 90-95 DEG C in packaging material, obtain lip gloss.
Test 5 groups:
Hydrogenated polydecene, tridecyl alcohol trimellitate, two-two glycerol many acyl groups adipate esters-2, Fructus oleae europaeae fruit oil, squalane, behenyl alcohol, Jojoba seed oil, polyethylene, tocopherol acetas, bisabolol, farnesol are mixed and heated to 90-95 DEG C and melt completely; Add dimetylsilyl SiClx stone, complete with homogenizer homogenizing; Add polymethylsilsesquioxane, CI12490, dispersed with stirring is complete; Be filled to when 90-95 DEG C in packaging material, obtain lip gloss.
Test method: get above-mentioned different lip gloss, irradiate under being placed on D65 illumination, observes fading time.
Result of the test: in table 2.
The fading time of the different lip gloss of table 2
Note: enterprise marks: lip gloss faded defective lower than 5 days.
Conclusion (of pressure testing): above-mentioned test shows, the weight ratio of bisabolol and farnesol has most important for the quality of lip gloss, when the proportionate relationship of the two is 1:1, starts the longest of the time of fading, absolutely prove, select the part by weight relation of bisabolol and golden Flos Nelumbinis alcohol to have scientific meaning.
Preparation embodiment
Embodiment 1
Hydrogenated polydecene, tridecyl alcohol trimellitate, two-two glycerol many acyl groups adipate esters-2, Fructus oleae europaeae fruit oil, squalane, behenyl alcohol, Jojoba seed oil, polyethylene, tocopherol acetas, bisabolol, farnesol are mixed and heated to 90-95 DEG C and melt completely; Add dimetylsilyl SiClx stone, complete with homogenizer homogenizing; Add polymethylsilsesquioxane, CI12490, dispersed with stirring is complete; Be filled to when 90-95 DEG C in packaging material, obtain lip gloss.
Embodiment 2
Hydrogenated polydecene, tridecyl alcohol trimellitate, two-two glycerol many acyl groups adipate esters-2, Fructus oleae europaeae fruit oil, squalane, behenyl alcohol, Jojoba seed oil, polyethylene, tocopherol acetas, bisabolol, farnesol are mixed and heated to 90-95 DEG C and melt completely; Add dimetylsilyl SiClx stone, complete with homogenizer homogenizing; Add polymethylsilsesquioxane, CI12490, dispersed with stirring is complete; Be filled to when 90-95 DEG C in packaging material, obtain lip gloss.
Embodiment 3
Hydrogenated polydecene, tridecyl alcohol trimellitate, two-two glycerol many acyl groups adipate esters-2, Fructus oleae europaeae fruit oil, squalane, behenyl alcohol, Jojoba seed oil, polyethylene, tocopherol acetas, bisabolol, farnesol are mixed and heated to 90-95 DEG C and melt completely; Add dimetylsilyl SiClx stone, complete with homogenizer homogenizing; Add polymethylsilsesquioxane, CI12490, dispersed with stirring is complete; Be filled to when 90-95 DEG C in packaging material, obtain lip gloss.
The requirement all meeting quality standard of above-described embodiment lip gloss.
Preparation embodiment includes but not limited to above-mentioned.

Claims (10)

1. a lip gloss, is prepared from by emollient, skin conditioning agent, thickening agent, antioxidant and coloring agent, and it is characterized in that coloring agent is made up of polymethylsilsesquioxane and CI12490, skin conditioning agent comprises bisabolol and farnesol.
2. a kind of lip gloss according to claim 1, wherein emollient 100-110 weight portion, skin conditioning agent 9-13 weight portion, thickening agent 8-10 weight portion, antioxidant 1-1.5 weight portion, coloring agent 1.5-2.5 weight portion.
3. a kind of lip gloss according to claim 1, wherein emollient 105 weight portion, skin conditioning agent 11 weight portion, thickening agent 9 weight portion, antioxidant 1.2 weight portion, coloring agent 2 weight portion.
4. a kind of lip gloss according to claim 1, wherein the weight ratio of polymethylsilsesquioxane and CI12490 is 1.98:0.02.
5. a kind of lip gloss according to claim 1, wherein bisabolol and farnesol weight ratio are 1:1.
6. a kind of lip gloss according to claim 1, wherein emollient is hydrogenated polydecene, tridecyl alcohol trimellitate, two-two glycerol many acyl groups adipate esters-2, Fructus oleae europaeae fruit oil, behenyl alcohol.
7. a kind of lip gloss according to claim 1, wherein skin conditioning agent squalane, Jojoba seed oil.
8. a kind of lip gloss according to claim 1, wherein thickening agent dimetylsilyl SiClx stone, polyethylene.
9. a kind of lip gloss according to claim 1, wherein anti-oxidant tocopherol acetas, butylated hydroxytoluene.
10. a kind of lip gloss according to any one of claim 1-9, wherein the preparation method of cosmetics is:
Hydrogenated polydecene, tridecyl alcohol trimellitate, two-two glycerol many acyl groups adipate esters-2, Fructus oleae europaeae fruit oil, squalane, behenyl alcohol, Jojoba seed oil, polyethylene, tocopherol acetas, bisabolol, farnesol are mixed and heated to 90-95 DEG C and melt completely; Add dimetylsilyl SiClx stone, complete with homogenizer homogenizing; Add polymethylsilsesquioxane, CI12490, dispersed with stirring is complete; Be filled to when 90-95 DEG C in packaging material, obtain lip gloss.
CN201510642689.2A 2015-09-29 2015-09-29 A kind of permanent color lip gloss and preparation method thereof Active CN105250159B (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107375002A (en) * 2017-08-25 2017-11-24 漳浦彩露华化妆品有限公司 One kind dazzles color lip gloss and preparation method thereof
CN107468530A (en) * 2017-08-25 2017-12-15 漳浦彩露华化妆品有限公司 A kind of liquid lipstick and preparation method thereof
CN107951741A (en) * 2017-10-31 2018-04-24 廖烈武 A kind of not de- adornment lipstick and preparation method thereof
CN108938497A (en) * 2018-09-21 2018-12-07 娇时日化(杭州)股份有限公司 A kind of bloom rich in extracted form natural plant moistens solid lip gloss and its production technology
CN109044889A (en) * 2018-10-24 2018-12-21 娇时日化(杭州)股份有限公司 A kind of cloudy surface lipstick and its production technology that jade-like stone Rinsing is sliding

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1934168A (en) * 2004-03-16 2007-03-21 陶氏康宁公司 Alkyl-phenyl silsesquioxane resins compositions
US20100015071A1 (en) * 2007-02-27 2010-01-21 Biospectrum Inc. Compositions for Improving Skin Conditions Comprising Alpha-Bisabolol as an Active Ingredient
CN102973436A (en) * 2012-12-19 2013-03-20 珀莱雅化妆品股份有限公司 Making-up cosmetics composition with elastic touch
US20130272982A1 (en) * 2010-11-08 2013-10-17 Coty Inc. Shiny, transfer resistant lipstick and method of making

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1934168A (en) * 2004-03-16 2007-03-21 陶氏康宁公司 Alkyl-phenyl silsesquioxane resins compositions
US20100015071A1 (en) * 2007-02-27 2010-01-21 Biospectrum Inc. Compositions for Improving Skin Conditions Comprising Alpha-Bisabolol as an Active Ingredient
US20130272982A1 (en) * 2010-11-08 2013-10-17 Coty Inc. Shiny, transfer resistant lipstick and method of making
CN102973436A (en) * 2012-12-19 2013-03-20 珀莱雅化妆品股份有限公司 Making-up cosmetics composition with elastic touch

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107375002A (en) * 2017-08-25 2017-11-24 漳浦彩露华化妆品有限公司 One kind dazzles color lip gloss and preparation method thereof
CN107468530A (en) * 2017-08-25 2017-12-15 漳浦彩露华化妆品有限公司 A kind of liquid lipstick and preparation method thereof
CN107951741A (en) * 2017-10-31 2018-04-24 廖烈武 A kind of not de- adornment lipstick and preparation method thereof
CN108938497A (en) * 2018-09-21 2018-12-07 娇时日化(杭州)股份有限公司 A kind of bloom rich in extracted form natural plant moistens solid lip gloss and its production technology
CN109044889A (en) * 2018-10-24 2018-12-21 娇时日化(杭州)股份有限公司 A kind of cloudy surface lipstick and its production technology that jade-like stone Rinsing is sliding
CN109044889B (en) * 2018-10-24 2021-08-31 虞琼斐 Glossy and smooth matte lipstick and production process thereof

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Address after: Panyu District Hualong Town Guangzhou city Guangdong province 511434 Liu Wai Street No. 13 (No. 1 building)

Patentee after: Hua An Tang biotech Group Co., Ltd.

Address before: Panyu District Hualong Town Guangzhou city Guangdong province 511434 Liu Wai Street No. 13 (No. 1 building)

Patentee before: City flower An Tang bio tech ltd, Guangzhou

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