CN102964935A - Environment-friendly inorganic antifouling mouldproof odorless wall paint and preparation method thereof - Google Patents
Environment-friendly inorganic antifouling mouldproof odorless wall paint and preparation method thereof Download PDFInfo
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- CN102964935A CN102964935A CN2012104915138A CN201210491513A CN102964935A CN 102964935 A CN102964935 A CN 102964935A CN 2012104915138 A CN2012104915138 A CN 2012104915138A CN 201210491513 A CN201210491513 A CN 201210491513A CN 102964935 A CN102964935 A CN 102964935A
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Abstract
The invention relates to the technical field of coating and particularly relates to antifouling mouldproof odorless inorganic wall paint. The antifouling mouldproof odorless inorganic wall paint comprises a defoaming agent A, a dispersant A, a dispersant B, kaolin, a thickening agent, titanium dioxide, talcum powder, a pH regulator, calcium carbonate, an antifreeze agent, a coalescing agent, an antifoaming agent B, a mould inhibitor, a corrosion remover, styrene acrylic emulsion and potassium silicate. The materials are added at different times and prepared into a final product under the control of different mixing revolutions. The antifouling mouldproof odorless inorganic wall paint not only has excellent physical performance of inorganic coating, but also has excellent antifouling and mouldproof performance of organic coating, and does not have unpleasant smell simultaneously when being environment-friendly.
Description
Technical field
The present invention relates to technical field of coatings, particularly relate to a kind of environmental protection inorganic anti-soil mildew-resistant wall paint and preparation method thereof of only distinguishing the flavor of.
Background technology
Ubiquitous in our the occurring in nature microorganism of life, and its growth and breeding is rapid, and variation is fast, strong adaptability.In the building coating because being rich in the needed nutrient of microorganism growth and being fit to the environment (temperature, humidity and pH value etc.) of its growth, the easier growth and breeding of microorganism, produce thus the metabolites such as various enzymes, bacterium and toxin, make that paint film fades, variable color, the physical and mechanical property variation, both affect the wall body decoration effect, reduced again the work-ing life of filming.Therefore we need a kind of pollution resistance, all good products of mildew resistance.
For mould-repellant coating, its used base-material has inorganic base material and organic base-material (mainly being latex coating) two classes, and main relative merits are as follows:
(1), silicification reaction
Inorganic paint: be permeable to mineral substrate 0.5-2mm, produce silicification reaction with mineral substrate, formed afterwards the hard silica surface of alkali resistant acid-proof in 35-40 days and chemical combination together;
Latex coating: without silicification reaction, paint film is the surface adhesion of physical property, and cohesive force is different because of the contained ratio of polyester adhesive, is attached to building surface, is film like, easily comes off.
(2), color persistence
Inorganic paint: the natural inorganic oxidized metal is painted, although colour-fast, color is gorgeous not, and decorative effect is not ideal enough;
Latex coating: the synthetic organic pigment, although beautiful in colour, relative fugitive color.
(3), thermal expansivity
Inorganic paint: with mineral substrate identical dilation coefficient is arranged, but and reflection ray and thermal radiation, can avoid expanding with heat and contract with cold and the be full of cracks that produces and coming off
Latex coating: inconsistent with the dilation coefficient of mineral substrate, hot coefficient and metope differ 10-20 doubly, easily cause the be full of cracks that coating produces because expanding with heat and contract with cold and come off.
(4), alkali-resistivity
Inorganic paint: belong to alkalescence, the pH value is consistent with mineral substrate, without repellency, can directly brush, and can prevent the invasion and attack of body of wall alkalescence;
Latex coating: pH value and mineral substrate are inconsistent, and repellency is arranged, and must make alkali resistant priming paint, can't avoid the invasion and attack of body of wall alkalescence fully.
(5), ventilation property
Inorganic paint: have respiratory function, the moisture in the body of wall can freely outwards evaporate, and can prevent coating foaming, can guarantee that body of wall and coating are dry and comfortable;
Latex coating: coating is air-locked film, does not have a respiratory, and moisture can't outwards evaporate, and paint film can accumulate because of the moisture in the body of wall and bubbles too much, and come off.
(6), antibiotic and liver moss
Inorganic paint: inorganic components, do not contain nutrition, alkaline environment can be killed bryophyte spores, and coatingsurface is dry and comfortable without moisture;
Latex coating: organic composition, contain nutrition, the moss growth environment is provided, need to add except the moss agent, can be harmful to human body and environment.
(7), uninflammability
Inorganic paint: inorganic nature, do not burn under the high temperature and do not give out toxic gas;
Latex coating: organic components, easy firing, and may distribute toxic gas.
(8), anti-soil, resistance to acid
Inorganic paint: hard petrochemical industry surface is arranged, not resinous, be difficult for producing static, dust is not adsorbed in the invasion and attack of the acidic substance such as acid and alkali rain and industry or automobile exhaust gas;
Latex coating: resinous, easily produce static, the coatingsurface flintiness is low, easily adsorbs dust, meets easily efflorescence of acid.
(9), workability
Inorganic paint: only need brushing to get final product for twice, construction is simple;
Latex coating: do first the alkali resistant bottom, brush again finish paint twice; The alkali resistant bottom must be with the body of wall complete closed, otherwise can cause the variable color of finish paint and come off the technique relative complex.
On the whole, inorganic paint has comparatively significantly advantage at physical properties, and it does not provide microorganism growth needed nutrient, and anti-mold effect is relatively excellent, but decorative effect is desirable not to the utmost.And organic coating is because being rich in the required nutrient of microorganism growth and environment, and therefore the inorganic paint anti-mold effect is poor relatively.
Pursuing best performance is the direction of always effort of people, but does not also have to take into account at present the mould-repellant coating of inorganic and organic all respects premium properties.
Summary of the invention
For addressing the above problem, the object of the invention is to, provide a kind of not only physical properties good, and the inorganic wall paint of the clean flavor of the environment-friendly type anti-soil mildew-resistant of anti-soil anti-mold effect excellence.
Two of purpose of the present invention provides the preparation method of the inorganic wall paint of the clean flavor of described environment-friendly type anti-soil mildew-resistant
The present invention is achieved through the following technical solutions:
The inorganic wall paint of the clean flavor of a kind of environment-friendly type anti-soil mildew-resistant is comprised of the following material that calculates according to weight percent:
Wherein, defoamer A is for pressing down the alveolitoid mineral oil antifoam agent, preferred Blackburn CF439; Defoamer B is broken alveolitoid mineral oil antifoam agent, preferred Blackburn CF246; Dispersant A is that mass concentration is 20% sodium hexametaphosphate solution, and dispersant B is acrylic dispersants; Water is preferably used deionized water.
Preferably, described kaolin is 4000 order calcined kaolins; Described titanium dioxide is Rutile type Titanium Dioxide; Described talcum powder is 1250 order talcum powder; Described calcium carbonate is 700 order water-ground limestones.
Preferably, described mould inhibitor is butyl carbamic acid-3-iodo-2-propynyl ester (IBPC) and aluminium chlorohydroxide (BAC) composition;
Preferably, described thickening material is Natvosol.
Preferably, described potassium silicate is admittedly to contain 30% potassium silicate solution; Preferred Inocot 330.
Preferably, described benzene emulsion is clean flavor benzene emulsion; The solid power ECO 599 of preferred D-BASF peace.
Preferably, described antifreezing agent is propylene glycol.
Preferably, described film coalescence aid is ester alcohol; The preferred Kathon CG of described sanitas, described pH adjusting agent, preferred AMP-95.
Prepare the method for the inorganic wall paint of the clean flavor of described anti-soil mildew-resistant, comprise being prepared as follows step:
The solvent of steps A, the water with described amount, defoamer A, dispersant A and dispersant B 2～5% mixes, and stirs 3～8 minutes under 400～600rpm, obtains finely dispersed mixed slurry I;
Step B, add kaolin, thickening material, titanium dioxide, talcum powder, pH adjusting agent and calcium carbonate in the gained mixed slurry I in the steps A, and under 1000～1500rpm, stir 20～40 minutes, obtain finely dispersed mixed slurry II; Wherein, described thickening material needs slowly to add;
Step C, add antifreezing agent, film coalescence aid, 2/3 defoamer B, mould inhibitor and sanitas in the gained mixed slurry II in the step B, under 800～1200rpm, stirred 3～8 minutes, obtain finely dispersed mixed slurry III;
Step D, add benzene emulsion, potassium silicate and 1/3 defoamer B in the gained mixed slurry III in the step C, under 100～150rpm, stirred 10～20 minutes, obtain the inorganic wall paint of the clean flavor of anti-soil mildew-resistant; Being wire during wherein said potassium silicate stirs adds.
The present invention includes defoamer A, dispersant A, dispersant B, kaolin, thickening material, titanium dioxide, talcum powder, pH adjusting agent, calcium carbonate, antifreezing agent, film coalescence aid, defoamer B, mould inhibitor, sanitas, benzene emulsion and potassium silicate etc., above-mentioned substance adds at different time, and stirring prepares finished product under the control of difference stirring revolution.The present invention is through the screening to filler, filmogen and auxiliary agent thereof, make between each component proportioning in a certain amount of scope, utilize synergy mutual between each material, so that final product, not only has the good physicals of inorganic paint, and anti-soil, fungicidal properties with organic coating excellence, in the time of environmental protection without offending smell.Wherein adopt take inorganic as main, organic is that auxiliary compound base-material comes component design, taken into account the advantage of inorganic paint and organic coating, in prescription, select ultralow VOC, formaldehyde content, and the organic benzene emulsion base-material of the clean flavor that does not contain APEO comes and the collocation of inorganic silicate base-material, and the finished product of making possesses high-dirt-resistance, long-acting mould-proof and excellent weathering resistance, water-repellancy, and is strong to the substrate cohesive force, scrub resistance is excellent, and performance is particularly outstanding in hot and humid and long-term moist environment.
Concrete embodiment
The present invention is described in further detail below in conjunction with embodiment, understands the present invention to help those skilled in the art.
Embodiment 1
The inorganic wall paint of the clean flavor of a kind of anti-soil mildew-resistant; Comprise the following material that calculates according to weight percent: defoamer A0.1%, dispersant A 0.8%, dispersant B 0.1%, kaolin 10%, thickening material 0.1%, titanium dioxide 20%, talcum powder 5%, pH adjusting agent 0.3%, calcium carbonate 25%, antifreezing agent 0.5%, film coalescence aid 0.8%, defoamer B0.1%, mould inhibitor 0.8%, sanitas 0.1%, benzene emulsion 10%, potassium silicate 15% and water.
The preparation method of the inorganic wall paint of the clean flavor of described anti-soil mildew-resistant; Comprise and be prepared as follows step:
Steps A, the water with described amount, defoamer A, dispersant A and dispersant B mix, and stir 8 minutes under 400rpm, obtain finely dispersed mixed slurry I;
Step B, add kaolin, thickening material, titanium dioxide, talcum powder, pH adjusting agent and calcium carbonate in the gained mixed slurry I in the steps A, and under 1000rpm, stirred 40 minutes, obtain finely dispersed mixed slurry II; Wherein, described thickening material needs slowly to add;
Step C, add antifreezing agent, film coalescence aid, 2/3 defoamer B, mould inhibitor and sanitas in the gained mixed slurry II in the step B, under 800rpm, stirred 3 minutes, obtain finely dispersed mixed slurry III;
Step D, add benzene emulsion, potassium silicate and 1/3 defoamer B in the gained mixed slurry III in the step C, under 100rpm, stirred 20 minutes, obtain the inorganic wall paint of the clean flavor of anti-soil mildew-resistant; Being wire during wherein said potassium silicate stirs adds.
Embodiment 2
The inorganic wall paint of the clean flavor of a kind of anti-soil mildew-resistant; Comprise the following material that calculates according to weight percent: defoamer A0.3%, dispersant A 0.3%, dispersant B 0.5%, kaolin 5%, thickening material 0.5%, titanium dioxide 10%, talcum powder 10%, pH adjusting agent 0.1%, calcium carbonate 20%, antifreezing agent 1%, film coalescence aid 0.3%, defoamer B0.5%, mould inhibitor 0.3%, sanitas 0.3%, benzene emulsion 5%, potassium silicate 20% and water.
The preparation method of the inorganic wall paint of the clean flavor of described anti-soil mildew-resistant; Comprise and be prepared as follows step:
The solvent of steps A, the water with described amount, defoamer A, dispersant A and dispersant B mixes, and stirs 3 minutes under 600rpm, obtains finely dispersed mixed slurry I;
Step B, add kaolin, thickening material, titanium dioxide, talcum powder, pH adjusting agent and calcium carbonate in the gained mixed slurry I in the steps A, and under 1500rpm, stirred 20 minutes, obtain finely dispersed mixed slurry II; Wherein, described thickening material needs slowly to add;
Step C, add antifreezing agent, film coalescence aid, 2/3 defoamer B, mould inhibitor and sanitas in the gained mixed slurry II in the step B, under 1200rpm, stirred 3 minutes, obtain finely dispersed mixed slurry III;
Step D, add benzene emulsion, potassium silicate and 1/3 defoamer B in the gained mixed slurry III in the step C, under 150rpm, stirred 10 minutes, obtain the inorganic wall paint of the clean flavor of anti-soil mildew-resistant; Being wire during wherein said potassium silicate stirs adds.
Embodiment 3
The inorganic wall paint of the clean flavor of a kind of anti-soil mildew-resistant; Comprise the following material that calculates according to weight percent: defoamer A0.15%, dispersant A 0.5%, dispersant B 0.3%, kaolin 8%, thickening material 0.25%, titanium dioxide 16%, talcum powder 6%, pH adjusting agent 0.1%, calcium carbonate 21%, antifreezing agent 0.7%, film coalescence aid 0.5%, defoamer B0.3%, mould inhibitor 0.5%, sanitas 0.2%, benzene emulsion 8%, potassium silicate 18% and water.
The preparation method of the inorganic wall paint of the clean flavor of described anti-soil mildew-resistant; Comprise and be prepared as follows step:
The solvent of steps A, the water with described amount, defoamer A, dispersant A and dispersant B mixes, and stirs 5 minutes under 500rpm, obtains finely dispersed mixed slurry I;
Step B, add kaolin, thickening material, titanium dioxide, talcum powder, pH adjusting agent and calcium carbonate in the gained mixed slurry I in the steps A, and under 1200rpm, stirred 30 minutes, obtain finely dispersed mixed slurry II; Wherein, described thickening material needs slowly to add;
Step C, add antifreezing agent, film coalescence aid, 2/3 defoamer B, mould inhibitor and sanitas in the gained mixed slurry II in the step B, under 1000rpm, stirred 5 minutes, obtain finely dispersed mixed slurry III;
Step D, add benzene emulsion, potassium silicate and 1/3 defoamer B in the gained mixed slurry III in the step C, under 130rpm, stirred 15 minutes, obtain the inorganic wall paint of the clean flavor of anti-soil mildew-resistant; Being wire during wherein said potassium silicate stirs adds.
Embodiment 4
The inorganic wall paint of the clean flavor of a kind of anti-soil mildew-resistant; Comprise the following material that calculates according to weight percent: defoamer A0.2%, dispersant A 0.6%, dispersant B 0.2%, kaolin 6%, thickening material 0.4%, titanium dioxide 12%, talcum powder 8%, pH adjusting agent 0.2%, calcium carbonate 23%, antifreezing agent 0.6%, film coalescence aid 0.7%, defoamer B0.4%, mould inhibitor 0.7%, sanitas 0.2%, benzene emulsion 6%, potassium silicate 16% and water.
The preparation method of the inorganic wall paint of the clean flavor of described anti-soil mildew-resistant; Comprise and be prepared as follows step:
The solvent of steps A, the water with described amount, defoamer A, dispersant A and dispersant B mixes, and stirs 5 minutes under 500rpm, obtains finely dispersed mixed slurry I;
Step B, add kaolin, thickening material, titanium dioxide, talcum powder, pH adjusting agent and calcium carbonate in the gained mixed slurry I in the steps A, and under 1100rpm, stirred 30 minutes, obtain finely dispersed mixed slurry II; Wherein, described thickening material needs slowly to add;
Step C, add antifreezing agent, film coalescence aid, 2/3 defoamer B, mould inhibitor and sanitas in the gained mixed slurry II in the step B, under 1000rpm, stirred 6 minutes, obtain finely dispersed mixed slurry III;
Step D, add benzene emulsion, potassium silicate and 1/3 defoamer B in the gained mixed slurry III in the step C, under 120rpm, stirred 15 minutes, obtain the inorganic wall paint of the clean flavor of anti-soil mildew-resistant; Being wire during wherein said potassium silicate stirs adds.
Above-described embodiment is preferred embodiment of the present invention, is not to limit the scope of the present invention, so all equivalences of being done with the described feature of claim of the present invention and principle change or modify, all should be included within the claim scope of the present invention.
The present invention and existing coating are carried out concrete physical property measurement, and data are as follows:
Claims (9)
1. the inorganic wall paint of the clean flavor of environment-friendly type anti-soil mildew-resistant is characterized in that: be comprised of the following material that calculates according to weight percent:
Wherein, defoamer A is for pressing down the alveolitoid mineral oil antifoam agent, and defoamer B is broken alveolitoid mineral oil antifoam agent, and dispersant A is that mass concentration is 20% sodium hexametaphosphate solution, and dispersant B is acrylic dispersants.
2. the inorganic wall paint of the clean flavor of anti-soil mildew-resistant according to claim 1, it is characterized in that: described kaolin is 4000 order calcined kaolins, described titanium dioxide is Rutile type Titanium Dioxide, and described talcum powder is 1250 order talcum powder, and described calcium carbonate is 700 order water-ground limestones.
3. the inorganic wall paint of the clean flavor of anti-soil mildew-resistant according to claim 1, it is characterized in that: described mould inhibitor is the composition of butyl carbamic acid-3-iodo-2-propynyl ester and aluminium chlorohydroxide.
4. the inorganic wall paint of the clean flavor of anti-soil mildew-resistant according to claim 1, it is characterized in that: described thickening material is Natvosol.
5. the inorganic wall paint of the clean flavor of anti-soil mildew-resistant according to claim 1 is characterized in that: described potassium silicate is for admittedly containing 30% potassium silicate solution.
6. the inorganic wall paint of the clean flavor of anti-soil mildew-resistant according to claim 1, it is characterized in that: described benzene emulsion is clean flavor benzene emulsion.
7. the inorganic wall paint of the clean flavor of anti-soil mildew-resistant according to claim 1, it is characterized in that: described antifreezing agent is propylene glycol.
8. the inorganic wall paint of the clean flavor of anti-soil mildew-resistant according to claim 1, it is characterized in that: described film coalescence aid is ester alcohol.
9. the method for preparing the inorganic wall paint of the clean flavor of as claimed in claim 1 anti-soil mildew-resistant; It is characterized in that, comprise being prepared as follows step:
Steps A, the water with described amount, defoamer A, dispersant A and dispersant B mix, and stir 3～8 minutes under 400～600rpm, obtain finely dispersed mixed slurry I;
Step B, add kaolin, thickening material, titanium dioxide, talcum powder, pH adjusting agent and calcium carbonate in the gained mixed slurry I in the steps A, and under 1000～1500rpm, stir 20～40 minutes, obtain finely dispersed mixed slurry II; Wherein, described thickening material needs slowly to add;
Step C, add antifreezing agent, film coalescence aid, 2/3 defoamer B, mould inhibitor and sanitas in the gained mixed slurry II in the step B, under 800～1200rpm, stirred 3～8 minutes, obtain finely dispersed mixed slurry III;
Step D, add benzene emulsion, potassium silicate and 1/3 defoamer B in the gained mixed slurry III in the step C, under 100～150rpm, stirred 10～20 minutes, obtain the inorganic wall paint of the clean flavor of anti-soil mildew-resistant; Being wire during wherein said potassium silicate stirs adds.
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| CN105255288A (en) * | 2015-11-20 | 2016-01-20 | 广东梅雁吉祥实业投资股份有限公司 | Metal product antirust coating material |
| CN105542603A (en) * | 2016-01-27 | 2016-05-04 | 广东施彩涂料有限公司 | High-strength inorganic paint and preparation method thereof |
| CN109135467A (en) * | 2018-07-18 | 2019-01-04 | 成都虹润制漆有限公司 | composite coating and preparation method thereof |
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| CN110105829A (en) * | 2019-05-10 | 2019-08-09 | 曾凡海 | Antiultraviolet vapor-permeable type wall finiss |
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| CN110564189A (en) * | 2019-09-18 | 2019-12-13 | 重庆兴渝新材料研究院有限公司 | inorganic nano-coating and preparation method thereof |
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| CN115286938A (en) * | 2022-08-01 | 2022-11-04 | 中山多涂乐建材有限公司 | Water-based inorganic interior wall coating and preparation method thereof |
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